Crystallization Reactor

The crystallization reactor is a crystallization equipment that requires freezing water or refrigerant water to cool down sharply in the interlayer after the material is mixed and reacted. It is also a mixing reaction equipment in the domestic process of material mixing, heating, cooling, stirring, etc.

Due to different processes and media, it is common for materials to be flammable, explosive, highly toxic, and high-temperature and high-pressure. The mixing form, speed, heating and cooling requirements of the equipment are different. The explosion-proof and non-explosion-proof requirements of the machine are also different. Therefore, the equipment can be divided into normal pressure and pressure vessels, and the users who need it should provide fundamental uses.

Working Principle of Crystallization Reactor:

The crystallization reactor is a crystallization equipment that requires chilled water or refrigerant water to cool down sharply in the interlayer after the material is mixed and reacted. Cleaning without dead angle requirements to meet the process conditions.

Crystallization Reactor Model:

ZZKD Machinery has been focusing on research and development and crystallization reactors for many years. Crystallization reactors are one of our main products. After many upgrades, there are more and more models and types of crystallization reactors, and their functions are more and more perfect. The appearance is also different. changed a lot. At present, our crystallization reactors are divided into the following types: GF-10L, GF-20L, GF-30L, GF-50L, GF-100L.

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  GF-10L Crystallization Reactor

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  GF-50L Crystallization Reactor

Crystallization Reactor Structure:

The crystallization reactor can be divided into two types: 316L and 304 according to the user's process requirements for equipment selection. The inside and outside of the pipe are polished to Ra0.45, and the heating layer is divided into spiral belt and jacket type. The heating energy is divided into steam and electric heating to choose from. The insulation board is made of 304 material and filled with polyurethane foaming agent. Equipped with sight glass, stirring device, feeding hole, tank washing device, respirator, liquid medicine inlet, injection water inlet, return flow inlet, steam inlet, condensate outlet, cooling water inlet, outlet, material outlet, sewage discharge Port, sampling port, temperature measuring port, liquid level device.

·The inside and outside of the crystallization reactor tube is polished, and the heating layer is divided into spiral belt and jacket type. The heating energy is divided into steam and electric heating to choose from.

·The insulation board is made of 304 material and filled with polyurethane foaming agent.

·It is equipped with sight light, sight mirror, stirring device, feeding hole, tank washer, respirator, liquid medicine inlet, injection water inlet, return flow inlet, steam inlet, condensate outlet, cooling water inlet, outlet, material outlet, Sewage outlet, sampling port, temperature measuring port, liquid level device.

Crystallization Reactor Features:

1. It is made of imported 316L stainless steel, the inner wall is polished by electrolytic mirror, and the outer wall is made of 304 fully welded structure for heat preservation and electrolytic matte treatment.

2. A 0.2 μm hydrophobic vent filter is installed on the body of the crystallization reactor.

3. It can withstand high temperature sterilization at 121°C and is equipped with a hygienic pressure gauge.

4. The external connection of the crystallization reactor tank adopts sanitary chucks.

5. Equipped with temperature monitoring device, 2 sight glasses, cleaning ball and nitrogen inlet.

6. The shaft seal adopts a special sanitary mechanical seal to ensure that the material is not polluted.

7. The crystallization reactor can adopt frequency conversion speed control device, and the speed adjustment range of the stirring shaft is large.

Crystallization Reactor Case:

This product is used for hydrolysis, neutralization crystallization, distillation, evaporation, storage and other production links in pharmaceutical, chemical, food, light industry and other industries.

(1) Dissolving CBD oil in the crystallization reactor

Dissolve clarified CBD oil in pentane, ensuring that the vent/condenser of the jacketed vessel is connected to a suitable blower motor or fume hood to vent pentane vapors. Pentane boils at 36 °C. Pentane gives off a lot of vapor even at lower temperatures. , make sure the vessel condenser is cooled to -20 °C. Add pentane to CBD oil in a 1:2 ratio in a jacketed vessel. Turn on stirring and turn on the heating bath and set to 45 °C. Wait until the solution reaches 45 °C and all the oil has dissolved.

(2) Precipitation in crystallization reactor

Set the bath to 5 °C. Reduce stirring speed. As the solution cools, it becomes more viscous. Adjust the stirrer to keep the RPM above 120. CBD crystals will spontaneously form or "flush" out of the pentane solution. Continue to lower the temperature to at least -10 °C. The temperatures you use and how they change over time will change the crystal growth.

(3) The crystallization reactor collects CBD crystals

Once precipitation has ceased, flush or physically remove CBD crystals from the reactor. Vacuum filter the crystal/liquid slurry to remove the mother liquor from the CBD crystals. Rinse the crystals with ice-cold pentane to wash away impurities from the crystal surface. More rinsing with pentane improves poor color but reduces overall yield. Keeping the CBD and material cool during this step will help increase yield.

Why Choose Us

Professional reactor equipment manufacturer

ZZKDMachinery Equipment Co., Ltd. is a family integrating production and trade. Our main product is laboratory reactor equipment. Crystallization reactor is one of our main products for sale. Our crystallization reactor models are: GF -10L, GF-20L, GF-30L, GF-50L, GF-100L. At the same time, we can also customize according to your needs. The company has been established for more than ten years, providing equipment solutions for tens of thousands of enterprises and individuals at home and abroad, and has won unanimous praise from domestic and foreign customers.

Fast delivery

We have warehouses in Los Angeles in the United States, Valencia in Spain, and Thailand. We can choose the nearest warehouse for delivery according to the customer's geographical location, ensuring that the customer receives the goods quickly.

Perfect after-sales team

We provide a one-year warranty service for the products we sell. We have a professional after-sales team to deal with customers' after-sales problems, and can provide corresponding technical guidance through videos and other methods.

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